However, he ran out of steam at the crucial moment and lost the fourth-set tiebreak 7-0 in a 1-6, 6-4, 6-1, 7-6 defeat that sparked wild celebrations among the home support at the purpose-built indoor court at Seville's Olympic Stadium.
Nadal's victory, his 16th in 16 Davis Cup singles matches on his favoured surface, gave Spain an unassailable 3-1 lead in the best-of-five tie as the favourites secured their third title in four years.
It was their second Davis Cup final victory over Argentina following their success in Mar del Plata in 2008 and they also claimed the enormous trophy, known in Spanish as the 'salad bowl', by beating Czech Republic in Barcelona in 2009.
"This is a very good way of finishing after a long year," Nadal, who won just three singles titles in 2011, his fewest number in seven years, told a news conference, before announcing that he was not planning to play Davis Cup in 2012.
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